Technology Process of C29H24ClN3OS
There total 3 articles about C29H24ClN3OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
at 0 - 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Lawessons reagent / toluene / 12 h / Reflux
2: Potassium hexacyanoferrate(III) / water; ethanol / 2 h / 90 °C
3: N-ethyl-N,N-diisopropylamine; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane; tetrahydrofuran; ethyl acetate / 2 h / 0 - 20 °C
With
Lawessons reagent; Potassium hexacyanoferrate(III); 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Potassium hexacyanoferrate(III) / water; ethanol / 2 h / 90 °C
2: N-ethyl-N,N-diisopropylamine; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane; tetrahydrofuran; ethyl acetate / 2 h / 0 - 20 °C
With
Potassium hexacyanoferrate(III); 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate;