Technology Process of C21H21NO3
There total 8 articles about C21H21NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate;
In
toluene;
at 110 ℃;
for 22h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sulfuric acid / water / Heating / reflux
1.2: 0.75 h / 0 - 5 °C
1.3: 20 - 80 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 1.33 h / -78 - 20 °C
2.2: 2 h / -78 - 20 °C
3.1: mercury(II) diacetate / chloroform / 5 h / 40 °C
4.1: dmap / chloroform / 1.08 h / 20 - 80 °C
5.1: potassium carbonate / palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate / toluene / 22 h / 110 °C
With
dmap; sulfuric acid; mercury(II) diacetate; isopropylmagnesium chloride; potassium carbonate;
palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; chloroform; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 1.33 h / -78 - 20 °C
1.2: 2 h / -78 - 20 °C
2.1: mercury(II) diacetate / chloroform / 5 h / 40 °C
3.1: dmap / chloroform / 1.08 h / 20 - 80 °C
4.1: potassium carbonate / palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate / toluene / 22 h / 110 °C
With
dmap; mercury(II) diacetate; isopropylmagnesium chloride; potassium carbonate;
palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; chloroform; toluene;
