2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

Base Information

Chemical Name:2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose
CAS No.:42321-02-8
Molecular Formula:C₁₉H₂₅NO₇
Molecular Weight:379.41
Hs Code.:

Synonyms:2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

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Chemical Property of 2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

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Technology Process of 2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

There total 7 articles about 2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108-24-7
acetic anhydride

: 104430-62-8
1,6-Anhydro-2-azido-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

: 42321-02-8
2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane; for 1.5h; under 26252.1 Torr; Ambient temperature;
DOI:10.1002/jlac.198619860408

Reference yield:

: 55682-47-8
1,6-anhydro-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranose

: 42321-02-8
2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / CH₂Cl₂

2: H₂S / pyridine; H₂O / 24 h

3: pyridine / 12 h

With pyridine; hydrogen sulfide; sodium hydride; In pyridine; dichloromethane; water;
DOI:10.1002/1099-0690(200208)2002:16<2710::AID-EJOC2710>3.0.CO;2-8

Reference yield:

: 104430-61-7
(R)-2-(((1R,2S,3R,4R,5R)-4-azido-2-(benzyloxy)-6,8-dioxabicyclo[3.2.1]octan-3-yl)oxy)propanoic acid

: 42321-02-8
2-Acetamido-1,6-anhydro-4-O-benzyl-2-desoxy-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; diethyl ether / 1 h

2: 82 percent / H₂ / 10percent Pd/C / dioxane / 1.5 h / 26252.1 Torr / Ambient temperature

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; diethyl ether;
DOI:10.1002/jlac.198619860408