3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine

Base Information

Chemical Name:3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine
CAS No.:1262193-61-2
Molecular Formula:C₂₁H₂₂N₆O
Molecular Weight:374.445
Hs Code.:

Synonyms:3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine

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Chemical Property of 3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine

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Technology Process of 3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine

There total 2 articles about 3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.3%

: 1145786-45-3
[4-(4-methyl-1H-imidazol-1-yl)-3-(methyloxy)phenyl]boronic acid

: 1145786-44-2
4-methyl-1-[2-(methyloxy)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1H-imidazole

: 1262197-25-0
C₁₀H₁₁BrN₄

: 1262193-61-2
3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine

Guidance literature:: With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; for 16h; Inert atmosphere; Reflux;

Reference yield:

: 1145786-44-2
4-methyl-1-[2-(methyloxy)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1H-imidazole

: 1262197-25-0
C₁₀H₁₁BrN₄

: 1262193-61-2
3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-1-methyl-N-(2-methylphenyl)-1H-1,2,4-triazol-5-amine

: C₂₂H₂₂N₄O₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 16h;
DOI:10.1016/j.bmcl.2014.10.024