(Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

Base Information

Chemical Name:(Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline
CAS No.:1416917-53-7
Molecular Formula:C₂₄H₁₄I₂N₂
Molecular Weight:584.198
Hs Code.:

Synonyms:(Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

Suppliers and Price of (Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

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Technology Process of (Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

There total 5 articles about (Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 75163-16-5
2,3-bis(phenylethynyl)quinoxaline

: 1416917-53-7
(Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

Guidance literature:: With iodine; potassium carbonate; In dichloromethane; at 25 ℃; stereoselective reaction; Sealed tube;
DOI:10.1002/asia.201601085

Reference yield: 59.0%

: 75163-16-5
2,3-bis(phenylethynyl)quinoxaline

: 1416917-53-7
(Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

: (E)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

Guidance literature:: With iodine; In nitromethane; at 20 ℃; for 24h; Inert atmosphere; Darkness;
DOI:10.1016/j.tet.2012.10.098

Reference yield:

: C₈H₄BrIN₂

: 1416917-53-7
(Z)-3-iodo-1-(iodo(phenyl)methylene)-2-phenyl-1H-cyclopenta[b]quinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 0.5 h / 25 °C / Inert atmosphere; Sealed tube

2: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere; Sealed tube

3: iodine; potassium carbonate / dichloromethane / 25 °C / Sealed tube

With bis-triphenylphosphine-palladium(II) chloride; iodine; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: |Sonogashira Cross-Coupling / 2: |Sonogashira Cross-Coupling;
DOI:10.1002/asia.201601085