2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester

Base Information

Chemical Name:2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester
CAS No.:114827-83-7
Molecular Formula:C₂₄H₃₃NO₁₀
Molecular Weight:495.527
Hs Code.:

Synonyms:2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester

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Chemical Property of 2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester

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Technology Process of 2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester

There total 4 articles about 2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 83237-12-1
<(2S,3S)-3-<(4R)-2,2-dimethyl-1,3-dioxolan-4-yl>oxiran-2-yl>carboxylic acid

: diethyl N-2,4-dimethoxybenzylaminomalonate

: 114827-83-7
2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester

Guidance literature:: With dicyclohexyl-carbodiimide;
DOI:10.1246/cl.1987.1403

Reference yield:

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 114827-83-7
2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / NaH / dimethylsulfoxide / 20 h / Ambient temperature

3: aq. NaOH

4: 42 percent / dicyclohexylcarbodiimide

With sodium hydroxide; sodium hydride; dicyclohexyl-carbodiimide; In dimethyl sulfoxide;
DOI:10.1246/cl.1987.1403

Reference yield:

: 83237-12-1,114827-82-6
(2SR,3RS,4R)-2,3-epoxy-4,5-iopropylidenedioxypentanoic acid

: 114827-83-7
2-{(2,4-Dimethoxy-benzyl)-[(2S,3R)-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-oxiranecarbonyl]-amino}-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: aq. NaOH

3: 42 percent / dicyclohexylcarbodiimide

With sodium hydroxide; dicyclohexyl-carbodiimide;
DOI:10.1246/cl.1987.1403