5,10-dioxatricyclo[7.1.0.0^4,6]decane

Base Information

Chemical Name:5,10-dioxatricyclo[7.1.0.0^4,6]decane
CAS No.:19740-81-9
Molecular Formula:C₈H₁₂O₂
Molecular Weight:140.182
Hs Code.:

5,10-dioxatricyclo[7.1.0.0<sup>4,6</sup>]decane

Synonyms:5,10-dioxatricyclo[7.1.0.0^4,6]decane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,10-dioxatricyclo[7.1.0.0^4,6]decane

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Technology Process of 5,10-dioxatricyclo[7.1.0.0^4,6]decane

There total 11 articles about 5,10-dioxatricyclo[7.1.0.0^4,6]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

: 1552-12-1,111-78-4
1,5-cis,cis-cyclooctadiene

: 286-75-9,19740-81-9,57378-35-5
1,2:5,6-diepoxycyclooctane

Guidance literature:: With phosphoric acid; sulfuric acid; dihydrogen peroxide; sodium tungstate; Aliquat 336; In water; 1,2-dichloro-ethane; at 70 ℃; for 1h; pH=1.6; microwave irradiation;
DOI:10.1080/00397910500278479

Reference yield: 98.0%

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

: 286-75-9,19740-81-9,57378-35-5
1,2:5,6-diepoxycyclooctane

Guidance literature:: With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; In acetonitrile; tert-butyl alcohol; at 20 ℃; for 1h; Green chemistry;
DOI:10.1021/jo5003938

Reference yield: 86.7%

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

: 286-75-9,19740-81-9,57378-35-5
1,2:5,6-diepoxycyclooctane

: 73176-71-3,637-90-1,73176-86-0,1225194-35-3,1225194-65-9
5,6-epoxycyclooctene

Guidance literature:: With C₃₀H₂₅ClCoN₃OP; dihydrogen peroxide; 1-ethyl-3-methylimidazolium hexafluorophosphate; In water; at 20 ℃; for 2h; Green chemistry;
DOI:10.1016/j.crci.2013.12.004