C₃₂H₄₃NO₅Si

Base Information

Chemical Name:C₃₂H₄₃NO₅Si
CAS No.:1316279-02-3
Molecular Formula:C₃₂H₄₃NO₅Si
Molecular Weight:549.783
Hs Code.:

C<sub>32</sub>H<sub>43</sub>NO<sub>5</sub>Si

Synonyms:C₃₂H₄₃NO₅Si

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Chemical Property of C₃₂H₄₃NO₅Si

Chemical Property:

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Technology Process of C₃₂H₄₃NO₅Si

There total 1 articles about C₃₂H₄₃NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1139773-78-6
C₁₆H₂₅NO₅

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1316279-02-3
C₃₂H₄₃NO₅Si

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 17h;

Reference yield:

: 1316279-02-3
C₃₂H₄₃NO₅Si

: 1316279-07-8
C₃₁H₄₃NO₄Si

Guidance literature:: With methanol; lithium borohydride; In tetrahydrofuran; toluene; at -5 - 22 ℃; for 22h;

Reference yield:

: 1316279-02-3
C₃₂H₄₃NO₅Si

: 1316279-31-8
C₅₀H₈₅IO₁₁SSi₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: lithium borohydride; methanol / toluene; tetrahydrofuran / 22 h / -5 - 22 °C

2.1: dmap; triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: zinc / methanesulfonic acid / tetrahydrofuran / 12 h / Reflux

4.1: water; acetic acid / tetrahydrofuran / 2 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

6.1: toluene / 0.5 h / 100 °C

7.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 1 h / -23 - -18 °C

8.1: hydrogen fluoride / acetonitrile; water / 20 h / 20 °C

9.1: pyridine / dichloromethane / 1 h / -10 - 0 °C

10.1: sodium iodide / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 - 22 °C

11.1: triethylamine; nickel dichloride; chromium dichloride; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide / tetrahydrofuran / 20.5 h / 22 - 24 °C / Inert atmosphere

11.2: 1 h / 0 - 5 °C

12.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

12.2: 1 h

With pyridine; chromium dichloride; methanol; dmap; lithium borohydride; hydrogen fluoride; water; potassium hexamethylsilazane; Dess-Martin periodane; acetic acid; triethylamine; trifluoroacetic acid; sodium iodide; nickel dichloride; zinc; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide; methanesulfonic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 11.1: Nozaki-Hiyama-Kishi Coupling;