N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

Base Information

Chemical Name:N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane
CAS No.:204689-74-7
Molecular Formula:C₃₃H₅₄N₄O₂
Molecular Weight:538.817
Hs Code.:

N<sup>6</sup>,N<sup>10</sup>-dibenzyl-N<sup>1</sup>-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

Synonyms:N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

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Chemical Property of N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

Chemical Property:

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Technology Process of N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

There total 9 articles about N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: N¹,N⁴-dibenzyl-N⁹-(tert-butoxycarbonyl)-N¹-(6-phthaloylhexyl)-4-aza-1,9-diaminononane

: 204689-74-7
N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

Guidance literature:: With hydrazine; In methanol; Heating;
DOI:10.1023/A:1011988317683

Reference yield:

: 51644-96-3
5-tert-butoxycarbonylamino-1-aminopentane

: 204689-74-7
N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

Guidance literature:: Multi-step reaction with 8 steps

1: MgSO₄ / methanol / 3 h

2: NaBH₄ / methanol / 19 h / Heating

3: 83.1 percent / 50 percent KF/Celite / acetonitrile / 15 h / Heating

4: 85.5 percent / N₂H₄ / methanol / 15 h / Heating

5: MgSO₄ / methanol

6: NaBH₄ / methanol / Heating

7: 65 percent / 50 percent KF/Celite / acetonitrile / Heating

8: 90 percent / N₂H₄ / methanol / Heating

With potassium fluoride; sodium tetrahydroborate; Celite; magnesium sulfate; hydrazine; In methanol; acetonitrile; 1: Condensation / 2: Reduction / 3: Alkylation / 4: dephthaloylation / 5: Condensation / 6: Reduction / 7: Alkylation / 8: dephthaloylation;
DOI:10.1023/A:1011988317683

Reference yield:

: 122631-98-5
N¹-benzyl-N⁵-(tert-butoxycarbonyl)-1,5-diaminopentane

: 204689-74-7
N⁶,N¹⁰-dibenzyl-N¹-(tert-butoxycarbonyl)-6,10-diaza-1,16-diaminohexadecane

Guidance literature:: Multi-step reaction with 6 steps

1: 83.1 percent / 50 percent KF/Celite / acetonitrile / 15 h / Heating

2: 85.5 percent / N₂H₄ / methanol / 15 h / Heating

3: MgSO₄ / methanol

4: NaBH₄ / methanol / Heating

5: 65 percent / 50 percent KF/Celite / acetonitrile / Heating

6: 90 percent / N₂H₄ / methanol / Heating

With potassium fluoride; sodium tetrahydroborate; Celite; magnesium sulfate; hydrazine; In methanol; acetonitrile; 1: Alkylation / 2: dephthaloylation / 3: Condensation / 4: Reduction / 5: Alkylation / 6: dephthaloylation;
DOI:10.1023/A:1011988317683