2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside
CAS No.:88261-74-9
Molecular Formula:C₃₂H₃₅NO₁₀
Molecular Weight:593.631
Hs Code.:

Synonyms:2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside

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Chemical Property of 2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside

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Technology Process of 2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside

There total 3 articles about 2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 100-27-6
2-(4-nitrophenyl)ethanol

: 88261-73-8
2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranosyl chloride

: 88261-74-9
2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: With silver(I) 4-methylbenzenesulfonate; for 6h; Ambient temperature;
DOI:10.1016/0008-6215(83)88407-9

Reference yield:

: 4,6-di-O-benzyl-D-mannopyranose

: 88261-74-9
2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / pyridine / Ambient temperature

2: 86 percent / HCl / diethyl ether / 6 h / Ambient temperature

3: 82 percent / silver p-toluenesulfonate / 6 h / Ambient temperature

With pyridine; hydrogenchloride; silver(I) 4-methylbenzenesulfonate; In diethyl ether;
DOI:10.1016/0008-6215(83)88407-9

Reference yield:

: 88261-71-6
1,2,3-Tri-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranose

: 88261-74-9
2-(4-nitrophenyl)ethyl 2,3-di-O-acetyl-4,6-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / HCl / diethyl ether / 6 h / Ambient temperature

2: 82 percent / silver p-toluenesulfonate / 6 h / Ambient temperature

With hydrogenchloride; silver(I) 4-methylbenzenesulfonate; In diethyl ether;
DOI:10.1016/0008-6215(83)88407-9