methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate

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Chemical Name:methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate
CAS No.:1264295-39-7
Molecular Formula:C₂₄H₂₁F₃N₄O₂
Molecular Weight:454.452
Hs Code.:

Synonyms:methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate

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Chemical Property of methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate

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Technology Process of methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate

There total 6 articles about methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6804-53-1
4-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-amine

: 1264296-41-4
methyl 2-benzyl-4-(diethoxyphosphoryl)-2-methyl-3-oxopentanoate

: 1264295-39-7
methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate

Guidance literature:: 4-(4-(trifluoromethyl)phenyl)-1H-pyrazol-5-amine; With acetic acid; sodium nitrite; In water; for 0.166667h;

With sodium carbonate; In water; pH=> 8;

methyl 2-benzyl-4-(diethoxyphosphoryl)-2-methyl-3-oxopentanoate; In dichloromethane; water; for 6h;

Reference yield:

: 210691-47-7
methyl 2-benzyl-3-oxo-pentanoate

: 1264295-39-7
methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 24 h / Reflux

2.1: bromine; acetic acid / 2 h / 20 °C

3.1: toluene / 18 h / 130 °C

4.1: sodium nitrite; acetic acid / water / 0.17 h

4.2: pH > 8

4.3: 6 h

With bromine; potassium carbonate; acetic acid; sodium nitrite; In water; toluene; acetonitrile;

Reference yield:

: 30414-53-0
methyl propanoyl acetate

: 1264295-39-7
methyl 2-methyl-2-(3-methyl-8-(4-(trifluoromethyl)phenyl)pyrazolo[5,1-c][1,2,4]triazin-4-yl)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 72 h

2.1: potassium carbonate / acetonitrile / 24 h / Reflux

3.1: bromine; acetic acid / 2 h / 20 °C

4.1: toluene / 18 h / 130 °C

5.1: sodium nitrite; acetic acid / water / 0.17 h

5.2: pH > 8

5.3: 6 h

With bromine; potassium carbonate; acetic acid; sodium nitrite; In water; toluene; acetonitrile;