{(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride}

Base Information

• Chemical Name: {(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride}
• CAS No.: 156398-90-2
• Molecular Formula: C₃₀H₂₈Cl₂N₂Zn
• Molecular Weight: 552.862
• Mol file: 156398-90-2.mol

Synonyms:{(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride}

Chemical Property of {(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of {(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride}

There total 1 articles about {(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,4,6-trimethylaniline (88-05-1) + zinc(II) chloride (7646-85-7,24359-56-6) + acenaphthene quinone (82-86-0) → {(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride} (156398-90-2)

Guidance literature:

In acetic acid; mixt. of acenaphthenequinone, ZnCl2 and 2,4,6-trimethylaniline in CH3COOH heated under reflux (80°C) for 1 h; cooled to room temp.; filtered off; washed (CH3COOH, Et2O); dried (air);

DOI:10.1016/j.molstruc.2004.01.040

Reference yield: 73.0%

{(bis(2,4,6-trimethylphenylimino)acenaphthene)zinc chloride} (156398-90-2) → bis[N-(2,4,6-trimethylphenyl)imino]acenaphthene

Guidance literature:

With sodium oxalate; In dichloromethane; Inert atmosphere;

DOI:10.1002/chem.201804811

upstream raw materials:

2,4,6-trimethylaniline

zinc(II) chloride

acenaphthene quinone