(R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

Base Information

Chemical Name:(R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide
CAS No.:1032192-17-8
Molecular Formula:C₂₀H₂₀F₃NO₃
Molecular Weight:379.379
Hs Code.:

Synonyms:(R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

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Chemical Property of (R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

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Technology Process of (R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

There total 3 articles about (R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1032191-90-4
((Z)-4-(benzyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

: 1032192-17-8
(R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

Guidance literature:: With bis(di-μ-chloro-μ-{[bis-η⁵-(4'R,5'R)-(S_p)-2-(2'-4',5'-dihydro-4',5'-diphenyl-1'-tosyl-imidazolyl)cyclopentadienyl] iron(II) 1-C,3'-N} dipalladium(II)); silver(I) 4-methylbenzenesulfonate; In chloroform; at 55 ℃; for 72h; optical yield given as %ee; Inert atmosphere; Darkness;
DOI:10.1002/chem.200701642

Reference yield: 93.0%

: C₂₀H₂₀F₃NO₃

: 1032192-17-8
(R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

Guidance literature:: With di-μ-chlorobis{(S-2-dimethylaminoethylphenyl-C1,N)palladium(II)}; Ag-(S)-TRIP; In chloroform; at 20 - 35 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Darkness;
DOI:10.1002/anie.201103843

Reference yield:

: 1032191-90-4
((Z)-4-(benzyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

: 1032192-17-8
(R)-N-(1-(benzyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

: C₂₀H₂₀F₃NO₃

Guidance literature:: With C₁₀₈H₈₈Cl₄Fe₂N₈O₈Pd₂Pt₂S₄; C₁₀₈H₈₈Cl₄Fe₂N₈O₈Pd₂Pt₂S₄; silver(I) 4-methylbenzenesulfonate; In chloroform; at 55 ℃; for 72h; Reagent/catalyst; Overall yield = 94 %; enantioselective reaction; Catalytic behavior; Inert atmosphere; Sealed tube;
DOI:10.1021/om300600v