2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane

Base Information

Chemical Name:2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane
CAS No.:235092-95-2
Molecular Formula:C₄₈H₆₈N₄O₁₂S₄
Molecular Weight:1021.35
Hs Code.:

Synonyms:2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane

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Chemical Property of 2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane

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Technology Process of 2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane

There total 4 articles about 2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 235092-99-6
N,N'-propylenedioxybis(2,4,6-trimethylbenzenesulfonamide)

: 235093-02-4
N,N'-Bis(3-hydroxyethyl)-1,3-bis[(2-mesitylsulfonyl)aminooxy]propane

: 235092-95-2
2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1055/s-1999-6066

Reference yield: 45.0%

: 5469-66-9
propane-1,3-diol ditosylate

: 235092-99-6
N,N'-propylenedioxybis(2,4,6-trimethylbenzenesulfonamide)

: N²,N⁶-Bis(2-mesitylsulfonyl)-1,7-dioxa-2,6-diazacyclodecane

: 235092-95-2
2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1055/s-1999-6066

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 235092-95-2
2,6,12,16-tetrakis-(2,4,6-trimethyl-benzenesulfonyl)-1,7,11,17-tetraoxa-2,6,12,16-tetraaza-cycloeicosane

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine / 24 h / 20 °C

2: 37 percent / K₂CO₃ / dimethylformamide / 48 h / 20 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide; 1: Substitution / 2: Alkylation;
DOI:10.1055/s-1999-6066