C₁₉H₃₁NO₇Si

Base Information

Chemical Name:C₁₉H₃₁NO₇Si
CAS No.:1315455-08-3
Molecular Formula:C₁₉H₃₁NO₇Si
Molecular Weight:413.543
Hs Code.:

C<sub>19</sub>H<sub>31</sub>NO<sub>7</sub>Si

Synonyms:C₁₉H₃₁NO₇Si

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Chemical Property of C₁₉H₃₁NO₇Si

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Technology Process of C₁₉H₃₁NO₇Si

There total 7 articles about C₁₉H₃₁NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1315455-07-2
C₁₇H₂₉NO₆Si

: 78-39-7
Triethyl orthoacetate

: 1315455-08-3
C₁₉H₃₁NO₇Si

Guidance literature:: C₁₇H₂₉NO₆Si; Triethyl orthoacetate; With pyridinium p-toluenesulfonate; In water; benzene; at 20 ℃; for 0.166667h; Inert atmosphere;

With acetic acid; In water; benzene; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: 1021493-52-6
C₉H₆F₃NO₇S

: 1315455-08-3
C₁₉H₃₁NO₇Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate / methanol / 1.25 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane / 19.5 h / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 27.5 h / 80 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / tetrahydrofuran; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

4.2: 4 h / 20 °C

5.1: pyridinium p-toluenesulfonate / water; benzene / 0.17 h / 20 °C / Inert atmosphere

5.2: 0.17 h / 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/chem.201003489

Reference yield:

: 1315455-04-9
C₉H₈F₃NO₇S

: 1315455-08-3
C₁₉H₃₁NO₇Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / dichloromethane / 19.5 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 27.5 h / 80 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

3.2: 4 h / 20 °C

4.1: pyridinium p-toluenesulfonate / water; benzene / 0.17 h / 20 °C / Inert atmosphere

4.2: 0.17 h / 20 °C / Inert atmosphere

With 1H-imidazole; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/chem.201003489