methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:89756-12-7
Molecular Formula:C₃₁H₂₇NO₁₀
Molecular Weight:573.556
Hs Code.:

Synonyms:methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

Suppliers and Price of methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

There total 9 articles about methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 97242-75-6
methyl 3-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 89756-12-7
methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: benzoylation;
DOI:10.1016/S0040-4020(01)96688-8

Reference yield:

: 76101-14-9
methyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

: 89756-12-7
methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: TsOH*H₂O / acetonitrile / 16 h / 20 °C

2: pyridine / 16 h / 20 °C

3: Py*HClO₄ / nitromethane; methanol / 3 h / Heating

4: pyridine / 0.25 h

With pyridinium perchlorate; toluene-4-sulfonic acid; In pyridine; methanol; nitromethane; acetonitrile;
DOI:10.1007/BF01142798

Reference yield:

: 70831-94-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide

: 89756-12-7
methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / 20 °C / several hours

2: 100 percent / TsOH_.H₂O / acetonitrile / 16 h / 20 °C

3: acylation

4: pyridinium perchlorate, MeOH / nitromethane / 3 h / Heating

5: 83 percent / benzoylation

With methanol; pyridinium perchlorate; toluene-4-sulfonic acid; In nitromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)96688-8