{Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)}ClO₄

Base Information

• Chemical Name: {Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)}ClO₄
• CAS No.: 90486-04-7
• Molecular Formula: C₃₉H₃₀ClF₄N₄PRh*ClO₄
• Molecular Weight: 899.47

Synonyms:{Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)}ClO₄

Chemical Property of {Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)}ClO₄

Chemical Property:

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Technology Process of {Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)}ClO₄

There total 1 articles about {Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

{Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)}ClO4 (90443-81-5) → {Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)}ClO4 (90486-04-7)

Guidance literature:

With PPh₃; In dichloromethane; CH2Cl2 soln. of PPh3 added to CH2Cl2 soln. of Rh complex (molar ratio 1:1), stirred for 25 min; concd. in vac., pptd. by ether, filtered off, washed with ether, air-dried, elem. anal.;

DOI:10.1016/S0277-5387(00)88052-3

upstream raw materials:

{Rh(tetrafluorobenzobarrelene)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)}ClO₄

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