C₂₈H₂₅ClN₂O₄S

Base Information

Chemical Name:C₂₈H₂₅ClN₂O₄S
CAS No.:1423689-72-8
Molecular Formula:C₂₈H₂₅ClN₂O₄S
Molecular Weight:521.037
Hs Code.:

C<sub>28</sub>H<sub>25</sub>ClN<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₈H₂₅ClN₂O₄S

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Chemical Property of C₂₈H₂₅ClN₂O₄S

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Technology Process of C₂₈H₂₅ClN₂O₄S

There total 10 articles about C₂₈H₂₅ClN₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.8%

: 1423700-89-3
C₂₀H₁₇NO₄S

: 13524-04-4,131864-71-6,132437-66-2,120466-66-2
(R)-1-(o-chlorophenyl)ethanol

: 1423689-72-8
C₂₈H₂₅ClN₂O₄S

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In toluene; at 80 ℃; for 3h;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423689-72-8
C₂₈H₂₅ClN₂O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

With dimethylsulfide borane complex; diphenyl phosphoryl azide; triethylamine; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; toluene;

Reference yield:

: 25062-46-8,40979-16-6,34158-73-1
4-bromobenzaldehyde oxime

: 1423689-72-8
C₂₈H₂₅ClN₂O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 2 h / 15 - 20 °C

2.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C

3.1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / 5 h / 80 °C

4.1: hydrogen / ethanol / 3 h / 20 °C

5.1: Lawessons reagent / dichloromethane / 20 °C

5.2: 24 h

6.1: sodium hydroxide / methanol; tetrahydrofuran / 20 °C

6.2: 0 °C / pH 4.0

7.1: chloro-trimethyl-silane / methanol / 3 h / 0 - 20 °C

8.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

With Lawessons reagent; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; N-chloro-succinimide; chloro-trimethyl-silane; diphenyl phosphoryl azide; hydrogen; sodium methylate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;