16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5⁽¹⁰⁾,6,8,13-hexaen-17a-one-14-ol

Base Information

• Chemical Name: 16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5⁽¹⁰⁾,6,8,13-hexaen-17a-one-14-ol
• CAS No.: 126960-40-5
• Molecular Formula: C₁₉H₂₀O₂S
• Molecular Weight: 312.433

Synonyms:16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5⁽¹⁰⁾,6,8,13-hexaen-17a-one-14-ol

Chemical Property of 16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5⁽¹⁰⁾,6,8,13-hexaen-17a-one-14-ol

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Technology Process of 16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5⁽¹⁰⁾,6,8,13-hexaen-17a-one-14-ol

There total 1 articles about 16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5⁽¹⁰⁾,6,8,13-hexaen-17a-one-14-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(1-naphthyl-methylthio)succinimide (89030-43-3) + dimedone (126-81-8) → 16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5(10),6,8,13-hexaen-17a-one-14-ol (126960-40-5)

Guidance literature:

With N-benzyl-trimethylammonium hydroxide; Yield given. Multistep reaction; 1.) benzene , t-butyl alcohol, 30 min, room temperature, 2.) 48h;

Reference yield: 92.0%

acetic anhydride (108-24-7) + 16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5(10),6,8,13-hexaen-17a-one-14-ol (126960-40-5) → 16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5(10),6,8,13-hexaen-17a-one-14-acetate (126960-41-6)

Guidance literature:

With pyridine; at 100 ℃; for 3h;

upstream raw materials:

N-(1-naphthyl-methylthio)succinimide

dimedone

Downstream raw materials:

16,16-dimethyl-12-thia-D-homo-8,14-secogona-1,3,5⁽¹⁰⁾,6,8,13-hexaen-17a-one-14-acetate

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