dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:1129412-97-0
Molecular Formula:C₆₅H₈₈N₄O₁₅Si
Molecular Weight:1193.52
Hs Code.:

dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

Synonyms:dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1129412-95-8
dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-4,6-O-isopropylidene-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1129412-97-0
dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1002/chem.200701165

Reference yield:

: 1129412-97-0
dimethylthexylsilyl 3-O-[(R)-3-benzyloxy-dodecanoyl]-2-deoxy-2-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyl-(1->6)-3-O-allyloxycarbonyl-2-azido-4-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1032253-85-2
benzyl 3-deoxy-4,5-di-O-isopropylidene-7,8-di-O-benzyl-α,β-D-manno-2-octulopyranosyl fluoride

: C₉₇H₁₂₂N₄O₂₂Si

: 1129412-98-1
C₉₇H₁₂₂N₄O₂₂Si

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 1h; Title compound not separated from byproducts.;
DOI:10.1002/chem.200701165