3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole

Base Information

• Chemical Name: 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole
• CAS No.: 1152333-29-3
• Molecular Formula: C₂₉H₃₂N₄O₁₀S
• Molecular Weight: 628.66

Synonyms:3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole

Chemical Property of 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole

Chemical Property:

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Technology Process of 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole

There total 1 articles about 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

C15H14N4OS (111290-75-6) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole (1152333-29-3)

Guidance literature:

C₁₅H₁₄N₄OS; With potassium hydroxide; In ethanol; at 20 ℃; for 0.5h;

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide; In ethanol; at 20 ℃; for 48h;

DOI:10.1002/jccs.200800124

Reference yield: 92.0%

3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-ethoxyphenyl-4H-1,2,4-triazole (1152333-29-3) → C21H24N4O6S (1152333-43-1)

Guidance literature:

With methanol; ammonia;

DOI:10.1002/jccs.200800124

upstream raw materials:

C₁₅H₁₄N₄OS

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

Downstream raw materials:

C₂₁H₂₄N₄O₆S

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