13-deoxyanhydroaconitine

Base Information

Chemical Name:13-deoxyanhydroaconitine
CAS No.:99633-06-4
Molecular Formula:C₃₄H₄₅NO₉
Molecular Weight:611.733
Hs Code.:

Synonyms:13-deoxyanhydroaconitine

Suppliers and Price of 13-deoxyanhydroaconitine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 13-deoxyanhydroaconitine

Chemical Property:

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Technology Process of 13-deoxyanhydroaconitine

There total 2 articles about 13-deoxyanhydroaconitine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 99633-07-5
13-O-trifluoromethanesulfonylanhydroaconitine

: 99633-06-4
13-deoxyanhydroaconitine

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; water; for 3h; Irradiation;
DOI:10.1248/cpb.33.3658

Reference yield:

: 302-27-2,140188-61-0
aconitine

: 99633-06-4
13-deoxyanhydroaconitine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / pyridine / 18 h / Ambient temperature

2: 29 percent / hexamethylphosphoric acid triamide; H₂O / 3 h / Irradiation

In pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; water;
DOI:10.1248/cpb.33.3658