7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride

Base Information

Chemical Name:7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride
CAS No.:1263307-20-5
Molecular Formula:C₁₄H₉ClO₄S
Molecular Weight:308.742
Hs Code.:

Synonyms:7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride

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Chemical Property of 7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride

Chemical Property:

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Technology Process of 7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride

There total 3 articles about 7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1239973-29-5
ethyl 7-(chlorocarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carboxylate

: 1263307-20-5
7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 3.5 h / 10 - 20 °C

1.2: 0.17 h / Cooling

2.1: sodium hydroxide / ethanol / 3 h / Reflux

2.2: Acidic aq. solution

3.1: thionyl chloride / 3 h / Reflux

With aluminum (III) chloride; thionyl chloride; sodium hydroxide; In ethanol; dichloromethane; 1.1: Friedel Crafts acylation;
DOI:10.5012/bkcs.2010.31.11.3318

Reference yield:

: 154934-13-1
2,3-dihydro-thieno[3,4-b][1,4]dioxine-5,7-dicarboxylic acid diethyl ester

: 1263307-20-5
7-(phenylcarbonyl)-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbonyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / ethanol / 5 h / Reflux

1.2: 2 h / 60 °C

2.1: thionyl chloride / 5 h / Reflux

3.1: aluminum (III) chloride / dichloromethane / 3.5 h / 10 - 20 °C

3.2: 0.17 h / Cooling

4.1: sodium hydroxide / ethanol / 3 h / Reflux

4.2: Acidic aq. solution

5.1: thionyl chloride / 3 h / Reflux

With aluminum (III) chloride; thionyl chloride; sodium hydroxide; In ethanol; dichloromethane; 3.1: Friedel Crafts acylation;
DOI:10.5012/bkcs.2010.31.11.3318