1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene

Base Information

Chemical Name:1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene
CAS No.:99347-97-4
Molecular Formula:C₃₁H₃₆O₆
Molecular Weight:504.623
Hs Code.:

Synonyms:1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene

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Chemical Property of 1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene

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Technology Process of 1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene

There total 3 articles about 1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 99347-74-7
[1-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-benzyl)-2-methyl-allylsulfanyl]-acetic acid methyl ester

: 99347-97-4
1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 15 ℃; for 15h;
DOI:10.1248/cpb.33.1930

Reference yield:

: 66958-67-6
1,4-bis(benzyloxy)-2,3-dimethoxy-5-methyl-6-(3-methylbut-2-enyl)benzene

: 99347-97-4
1,4-dibenzyloxy-2,3-dimethoxy-6-<5-methoxycarbonyl-3-methyl-(2E)-penten-1-yl>-5-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CCl₄, -20 deg C, 20 min; 2.) DMF, 60 deg C, 20 h

2: 48 percent / NaH / dimethylsulfoxide / 15 h / 15 °C

With sodium hydride; In dimethyl sulfoxide;
DOI:10.1248/cpb.33.1930