N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin

Base Information

• Chemical Name: N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin
• CAS No.: 67565-30-4
• Molecular Formula: C₁₈H₁₄F₆N₂
• Molecular Weight: 372.313

Synonyms:N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin

Chemical Property of N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin

Chemical Property:

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Technology Process of N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin

There total 2 articles about N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N1-(2,6-dimethylphenyl)benzamidine (16239-27-3) + Hexafluoroacetone (684-16-2) → N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin (67565-30-4)

Guidance literature:

With pyridine; trichlorophosphate; In diethyl ether; at -15 ℃;

DOI:10.1016/S0022-1139(00)81451-7

Reference yield:

→ N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin (67565-30-4)

Guidance literature:

/BRN= 940075/, Hexafluoraceton, POCl3, Pyridin;

DOI:10.1055/s-1978-24796

Reference yield: 96.0%

N'-(2,6-Dimethylphenyl)-N-<2,2,2,-trifluor-1-(trifluormethyl)ethyliden>benzamidin (67565-30-4) + 1,2,3,4-tetrachloro-7,7-dimethoxy-5-phenylbicyclo[2.2.1]hepta-2,5-diene (1155-77-7) → 5,5-Dimethoxy-1-(2,6-dimethylphenyl)-2-phenyl-4,4-bis(trifluormethyl)-2-imidazolin

Guidance literature:

In toluene; at 125 ℃; for 3h;

DOI:10.1016/S0022-1139(00)81451-7

upstream raw materials:

N¹-(2,6-dimethylphenyl)benzamidine

Hexafluoroacetone

Downstream raw materials:

2.2-Dimethoxy-1-(2.6-dimethylphenyl)-2.5-diphenyl-3.3-bis(trifluormethyl)-2.2-dihydro-1.4.2-diazaphosphol-4-en

1-(2.6-Dimethylphenyl)-5-phenyl-3.3-bis(trifluormethyl)-2.2.2-trimethoxy-2.2-dihydro-1.4.2-diazaphosphol-4-en

1-(2.6-Dimethylphenyl)-5-phenyl-2.2.2-triethoxy-3.3-bis(trifluormethyl)-2.2-dihydro-1.4.2-diazaphosphol-4-en

7-(2.6-Dimethylphenyl)-6-methoxy-8-phenyl-10.10-bis(trifluormethyl)-1.5-dioxa-7.9-diaza-6-phosphaspiro<4.5>dec-8-en

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