C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃

Base Information

Chemical Name:C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃
CAS No.:85565-44-2
Molecular Formula:C₂₂H₃₂MoO₂
Molecular Weight:424.435
Hs Code.:

C<sub>5</sub>H<sub>4</sub>(C<sub>10</sub>H<sub>19</sub>)Mo(CO)2CH<sub>3</sub>CHCHCHCH<sub>3</sub>

Synonyms:C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃

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Chemical Property of C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃

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Technology Process of C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃

There total 1 articles about C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1809-26-3
2-bromopent-3-ene

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 85565-44-2
C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃

Guidance literature:: With lithium neomenthylcyclopentadienide; In tetrahydrofuran; acetonitrile; Mo(CO)6 suspn. in MeCN refluxing for 3 h under N2, ligand adding, solvent removing in vacuo, THF following by freshly prepared Li reagent adding, stirring for 10 h at 25°C., solvent removing, extg. with CH2Cl2-pentane and chromg. on Al2O3; purified by recrystn. from pentane; identified by elem. anal., IR and NMR spectra;
DOI:10.1021/ja00350a026

Reference yield: 80.0%

: 16921-91-8
nitrosyl hexafluorophosphate

: 85565-44-2
C₅H₄(C₁₀H₁₉)Mo(CO)2CH₃CHCHCHCH₃

: 85565-46-4
C₅H₄(C₁₀H₁₉)Mo(CO)(NO)CH₃CHCHCHCH₃⁽¹⁺⁾*PF₆^(1-)=C₅H₄(C₁₀H₁₉)Mo(CO)(NO)CH₃CHCHCHCH₃PF₆

Guidance literature:: In acetonitrile; byproducts: CO; Mo complex dissolving in MeCN at 0.degrtee.C under N2, nitrosonium saltadding to yield a dark-brown color and CO evolution; after 5 min at 0°C mixt. adding dropwise to cold ether, ppt. sepg. off by centrifugation; purified by recrystn. from CH2Cl2-pentane; identified by elem. anal., IR and NMR spectra;
DOI:10.1021/ja00350a026