8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

Base Information

Chemical Name:8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione
CAS No.:1338684-84-6
Molecular Formula:C₂₇H₃₁N₅O₃
Molecular Weight:473.575
Hs Code.:

Synonyms:8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

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Chemical Property of 8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

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Technology Process of 8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

There total 6 articles about 8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 141-91-3
2,6-dimethyl morpholine

: 1338684-85-7
8-(bromomethyl)-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

: 1338684-84-6
8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: 637-59-2
1-Bromo-3-phenylpropane

: 1338684-84-6
8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

1.2: 18 h / 20 °C

2.1: hydrogen / ethanol / 18 h / 20 °C / 760.05 Torr

3.1: boric acid; acetic acid / 18 h / 20 °C

4.1: dibenzoyl peroxide / 1,4-dioxane / 0.25 h / Inert atmosphere; Reflux

4.2: 48 h / Reflux

5.1: tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With hydrogen; boric acid; sodium hydride; acetic acid; dibenzoyl peroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 1338684-84-6
8-[(2,6-dimethylmorpholin-4-yl)methyl]-7-methyl-10-(3-phenylpropyl)benzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

1.2: 18 h / 20 °C

2.1: hydrogen / ethanol / 18 h / 20 °C / 760.05 Torr

3.1: boric acid; acetic acid / 18 h / 20 °C

4.1: dibenzoyl peroxide / 1,4-dioxane / 0.25 h / Inert atmosphere; Reflux

4.2: 48 h / Reflux

5.1: tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With hydrogen; boric acid; sodium hydride; acetic acid; dibenzoyl peroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide; mineral oil;