2-Sulfanyl-N,N'-di-isopropylisophthalamide

Base Information

Chemical Name:2-Sulfanyl-N,N'-di-isopropylisophthalamide
CAS No.:246230-42-2
Molecular Formula:C₁₄H₂₀N₂O₂S
Molecular Weight:280.391
Hs Code.:

Synonyms:2-Sulfanyl-N,N'-di-isopropylisophthalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Sulfanyl-N,N'-di-isopropylisophthalamide

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Technology Process of 2-Sulfanyl-N,N'-di-isopropylisophthalamide

There total 3 articles about 2-Sulfanyl-N,N'-di-isopropylisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 15088-33-2
N,N'-Di-isopropylisophthalamide

: 246230-42-2
2-Sulfanyl-N,N'-di-isopropylisophthalamide

Guidance literature:: N,N'-Di-isopropylisophthalamide; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -70 - 25 ℃; for 12h;

With sulfur; In tetrahydrofuran; hexane; at -60 - 20 ℃; for 49h;
DOI:10.1515/znb-1999-0812

Reference yield:

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 246230-42-2
2-Sulfanyl-N,N'-di-isopropylisophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 93 percent / CH₂Cl₂ / 2 h

2.1: BuLi; TMEDA / tetrahydrofuran; hexane / 12 h / -70 - 25 °C

2.2: 80 percent / sulfur / tetrahydrofuran; hexane / 49 h / -60 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; dichloromethane; 1.1: Acylation / 2.1: Metallation / 2.2: Substitution;
DOI:10.1515/znb-1999-0812