Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester

Base Information

Chemical Name:Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester
CAS No.:2374-76-7
Molecular Formula:C₄₂H₆₇N₃O₁₂
Molecular Weight:806.007
Hs Code.:

Synonyms:Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester

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Chemical Property of Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester

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Technology Process of Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester

There total 8 articles about Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2444-07-7
N-benzyloxycarbonyl-L-valine (R)-1-tert-butoxycarbonyl-2-methyl-propyl ester

: 2374-76-7
Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd-C / methanol; acetic acid

2: (i) SOCl₂, (ii) /BRN= 2417867/, Et₃N, Et₂O

3: CF₃CO₂H

4: (i) SOCl₂, (ii) /BRN= 2417867/, Et₃N, Et₂O

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In methanol; acetic acid;

Reference yield:

: 13498-71-0
L-Valyl-D-α-oxy-isovaleriansaeure-tert-butylester

: 2374-76-7
Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester

Guidance literature:: Multi-step reaction with 3 steps

1: (i) SOCl₂, (ii) /BRN= 2417867/, Et₃N, Et₂O

2: CF₃CO₂H

3: (i) SOCl₂, (ii) /BRN= 2417867/, Et₃N, Et₂O

With trifluoroacetic acid;

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 2374-76-7
Z-L-Valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleryl-L-valyl-D-α-oxy-isovaleriansaeure-tert.-butylester

Guidance literature:: Multi-step reaction with 5 steps

1: (i) PhSO₂Cl, Py, (ii) /BRN= 4658889/

2: H₂ / Pd-C / acetic acid

3: (i) PCl₅, Et₂O, (ii) /BRN= 2417867/, Et₃N

4: H₂ / Pd-C / ethanol

5: (i) PCl₅, Et₂O, (ii) /BRN= 2423139/, Et₃N

With hydrogen; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1007/BF00909454