2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside

Base Information

Chemical Name:2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside
CAS No.:882068-02-2
Molecular Formula:C₅₁H₅₀O₉Si
Molecular Weight:835.038
Hs Code.:

Synonyms:2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside

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Chemical Property of 2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside

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Technology Process of 2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside

There total 4 articles about 2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 195317-76-1
2-trimethylsilylethyl 2,3,4,6-tetra-O-acetyl-β-L-galactopyranoside

: 882068-02-2
2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / methanol / 4 h / 20 °C

2: 1.98 g / pyridine / 16 h / 50 °C

3: 3.52 g / pyridine / 3 h / 0 °C

With pyridine; sodium methylate; pyridine; In methanol;
DOI:10.1039/b513897c

Reference yield:

: 76-83-5
trityl chloride

: 882068-02-2
2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.98 g / pyridine / 16 h / 50 °C

2: 3.52 g / pyridine / 3 h / 0 °C

With pyridine; pyridine;
DOI:10.1039/b513897c

Reference yield:

: 198828-37-4
(2S,3S,4R,5S,6S)-2-Hydroxymethyl-6-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3,4,5-triol

: 882068-02-2
2-trimethylsilylethyl 6-O-triphenylmethyl-2,3,4-tri-O-benzoyl-β-L-galatopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.98 g / pyridine / 16 h / 50 °C

2: 3.52 g / pyridine / 3 h / 0 °C

With pyridine; pyridine;
DOI:10.1039/b513897c