3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

Base Information

Chemical Name:3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine
CAS No.:600553-70-6
Molecular Formula:C₃₁H₃₃ClN₄
Molecular Weight:497.083
Hs Code.:

Synonyms:3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

Suppliers and Price of 3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

There total 3 articles about 3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 600553-60-4
2-chloro-3-nitro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

: 600553-70-6
3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

Guidance literature:: With sodium tetrahydroborate; nickel dichloride; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1016/S0968-0896(03)00178-0

Reference yield:

: 5975-12-2
2,4-dichloro-3-nitro-pyridine

: 600553-70-6
3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Et₃N / dimethylformamide / 20 °C

2: 72 percent / NaBH₄ / NiCl₂*6H₂O / methanol; tetrahydrofuran / 20 °C

With sodium tetrahydroborate; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00178-0

Reference yield:

: 259180-74-0
2-(1-triphenylmethyl-4-piperidyl)ethylamine

: 600553-70-6
3-amino-2-chloro-4-[2-(1-triphenylmethyl-4-piperidyl)ethyl]aminopyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Et₃N / dimethylformamide / 20 °C

2: 72 percent / NaBH₄ / NiCl₂*6H₂O / methanol; tetrahydrofuran / 20 °C

With sodium tetrahydroborate; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00178-0