(3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

Base Information

Chemical Name:(3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid
CAS No.:1219835-21-8
Molecular Formula:C₂₆H₃₂N₂O₅S
Molecular Weight:484.616
Hs Code.:

Synonyms:(3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

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Chemical Property of (3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

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Technology Process of (3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

There total 1 articles about (3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1219835-18-3
(3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid methyl ester

: 1219835-21-8
(3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

Guidance literature:: (3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid methyl ester; With water; sodium hydroxide; In methanol; at 0 ℃; for 3h; under 750.075 Torr; pH=11; Inert atmosphere;

With potassium hydrogensulfate; In methanol; water; under 750.075 Torr; pH=7; Inert atmosphere;
DOI:10.1016/j.bmc.2010.01.009

Reference yield: 83.0%

: 1219835-21-8
(3S)-N-[Boc-S-(p-methylbenzyl)-L-cysteinyl]-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

: Cys(S-CH₂C₆H₄-Me-p)-OBzl

: 1219835-37-6
N-[(3S)-N-(Boc-S-(p-methylbenzyl)-L-cysteinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl]-S-(p-methylbenzyl)-L-cysteine benzyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 - 20 ℃; for 14h; under 750.075 Torr; pH=9; Inert atmosphere;
DOI:10.1016/j.bmc.2010.01.009