2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.0^3,8]nonadeca-1⁽¹⁹⁾,3⁽⁸⁾,4,6,15,17-hexaene 2-oxide

Base Information

• Chemical Name: 2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.0^3,8]nonadeca-1⁽¹⁹⁾,3⁽⁸⁾,4,6,15,17-hexaene 2-oxide
• CAS No.: 141874-83-1
• Molecular Formula: C₂₂H₂₁OPS₂
• Molecular Weight: 396.514

Synonyms:2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.0^3,8]nonadeca-1⁽¹⁹⁾,3⁽⁸⁾,4,6,15,17-hexaene 2-oxide

Chemical Property of 2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.0^3,8]nonadeca-1⁽¹⁹⁾,3⁽⁸⁾,4,6,15,17-hexaene 2-oxide

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Technology Process of 2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.0^3,8]nonadeca-1⁽¹⁹⁾,3⁽⁸⁾,4,6,15,17-hexaene 2-oxide

There total 1 articles about 2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.0^3,8]nonadeca-1⁽¹⁹⁾,3⁽⁸⁾,4,6,15,17-hexaene 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1,4-dibromo-butane (110-52-1) + C18H15OPS2 (119327-21-8) → 2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.03,8]nonadeca-1(19),3(8),4,6,15,17-hexaene 2-oxide (141874-83-1)

Guidance literature:

With potassium carbonate; In acetonitrile; Ambient temperature;

DOI:10.1016/0040-4039(92)88152-U

Reference yield:

2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.03,8]nonadeca-1(19),3(8),4,6,15,17-hexaene 2-oxide (141874-83-1) → (9R,14R)-2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.03,8]nonadeca-1(19),3(8),4,6,15,17-hexaene 2,9,14-trioxide (141874-84-2)

Guidance literature:

With dihydrogen peroxide; acetic acid; In dichloromethane; Ambient temperature;

DOI:10.1016/0040-4039(92)88152-U

upstream raw materials:

1,4-dibromo-butane

C₁₈H₁₅OPS₂

Downstream raw materials:

(9R,14R)-2-Phenyl-9,14-dithia-2-phospha-tricyclo[13.4.0.0^3,8]nonadeca-1⁽¹⁹⁾,3⁽⁸⁾,4,6,15,17-hexaene 2,9,14-trioxide

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