2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide

Base Information

• Chemical Name: 2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide
• CAS No.: 1238062-70-8
• Molecular Formula: C₂₅H₂₂N₆O₂
• Molecular Weight: 438.489

Synonyms:2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide

Chemical Property of 2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide

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Technology Process of 2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide

There total 1 articles about 2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

1‐methyl‐5‐aminomethylimidazole (486414-86-2) + 2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (1238062-69-5) → 2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide (1238062-70-8)

Guidance literature:

With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1016/j.bmc.2010.04.056

Reference yield:

2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide (1238062-70-8) → 2-(5-benzyl-1H-pyrazol-3-yl)-3-hydroxymethyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide (1238062-77-5)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2010.04.056

Reference yield:

morpholine (110-91-8,99108-56-2) + 2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide (1238062-70-8) → C29H31N7O2

Guidance literature:

With acetic acid; In methanol; at 20 ℃; for 12h;

DOI:10.1016/j.bmc.2010.04.056

upstream raw materials:

1‐methyl‐5‐aminomethylimidazole

2-(5-benzyl-1H-pyrazol-3-yl)-3-formyl-1H-indole-6-carboxylic acid

Downstream raw materials:

2-(5-benzyl-1H-pyrazol-3-yl)-3-hydroxymethyl-1H-indole-6-carboxylic acid (3-methyl-3H-imidazol-4-ylmethyl)-amide

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