methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate

Base Information

Chemical Name:methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate
CAS No.:797049-79-7
Molecular Formula:C₂₂H₃₄N₂O₅
Molecular Weight:406.522
Hs Code.:

Synonyms:methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate

Chemical Property:

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Technology Process of methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate

There total 2 articles about methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: methyl (S)-3-amino-5-methylhexanoate trifluoroacetic acid salt

: 215608-32-5
(R)-3-<(benzyoxycarbonyl)amino>-4-methylpentanoic acid

: 797049-79-7
methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1071/CH04080

Reference yield:

: 112121-72-9
Methyl (R)-(-)-N-benzyloxycarbonylamino-4-methylpentanoate

: 797049-79-7
methyl (3S,3'R)-3-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-5-methylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / tetrahydrofuran; H₂O / 3 h / 40 °C

2: 76 percent / BOP; iPr₂NEt / CH₂Cl₂

With potassium hydroxide; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1071/CH04080