1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane

Base Information

• Chemical Name: 1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane
• CAS No.: 1056675-67-2
• Molecular Formula: C₁₉H₂₂BrNO₂
• Molecular Weight: 376.293

Synonyms:1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane

Chemical Property of 1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane

Chemical Property:

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Technology Process of 1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane

There total 2 articles about 1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

1-tert-butoxycarbonylamino-1-(3-hydroxymethylphenyl)-(1R,S)-1-phenylmethane (1056675-63-8) → 1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane (1056675-67-2)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃;

Reference yield: 58.0%

→ 1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane (1056675-67-2)

Guidance literature:

Reference yield: 70.0%

(3S,5S)-5-((R)-1,2-dihydroxyethyl)-3-isopropyldihydrofuran-2(3H)-one (1056674-45-3) + 1-t(3-bromomethylphenyl)-1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethane (1056675-67-2) → 2,3-dideoxy-6-O-(3-(1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethyl)benzyl)-2-isopropyl-D-glucono-1,4-lactone (1056675-71-8)

Guidance literature:

With di(n-butyl)tin oxide; In toluene; regioselective reaction; Reflux;

DOI:10.1016/j.bmcl.2010.10.140

upstream raw materials:

1-tert-butoxycarbonylamino-1-(3-hydroxymethylphenyl)-(1R,S)-1-phenylmethane

Downstream raw materials:

2,3-dideoxy-6-O-(3-(1-tert-butoxycarbonylamino-(1R,S)-1-phenylmethyl)benzyl)-2-isopropyl-D-glucono-1,4-lactone

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