6-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-7-methyl-3-oxo-(9CI)

Base Information

Chemical Name:6-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-7-methyl-3-oxo-(9CI)
CAS No.:186666-77-3
Molecular Formula:C₁₀H₉N₃O
Molecular Weight:187.201
Hs Code.:
Mol file:186666-77-3.mol

Synonyms:6-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-7-methyl-3-oxo-(9CI);7-METHYL-3-OXO-1,2,3,4-TETRAHYDROQUINOXALINE-6-CARBONITRILE

Suppliers and Price of 6-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-7-methyl-3-oxo-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 6-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-7-methyl-3-oxo-(9CI)

Chemical Property:

PSA：64.92000
LogP:1.50668

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-7-methyl-3-oxo-(9CI)

There total 3 articles about 6-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-7-methyl-3-oxo-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 186666-75-1
N-(4-cyano-5-methyl-2-nitrophenyl)glycine

: 186666-77-3
7-Methyl-3-oxo-1,2,3,4-tetrahydro-quinoxaline-6-carbonitrile

Guidance literature:: With sodium dithionite; In water; at 100 ℃; for 1h;
DOI:10.1021/jm960654b

Reference yield:

: 50712-68-0
4-chloro-2-methylbenzonitrile

: 186666-77-3
7-Methyl-3-oxo-1,2,3,4-tetrahydro-quinoxaline-6-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: KNO₃, concd. H₂SO₄ / 0 - 20 °C

2: aq. ethanol / 48 h / Heating

3: 55 percent / Na₂S₂O₄ / H₂O / 1 h / 100 °C

With sodium dithionite; sulfuric acid; potassium nitrate; In ethanol; water;
DOI:10.1021/jm960654b

Reference yield:

: 178448-14-1
4-chloro-2-methyl-5-nitrobenzonitrile

: 186666-77-3
7-Methyl-3-oxo-1,2,3,4-tetrahydro-quinoxaline-6-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: aq. ethanol / 48 h / Heating

2: 55 percent / Na₂S₂O₄ / H₂O / 1 h / 100 °C

With sodium dithionite; In ethanol; water;
DOI:10.1021/jm960654b