C₂₁H₂₂NP

Base Information

Chemical Name:C₂₁H₂₂NP
CAS No.:1390631-77-2
Molecular Formula:C₂₁H₂₂NP
Molecular Weight:319.386
Hs Code.:

Synonyms:C₂₁H₂₂NP

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Chemical Property of C₂₁H₂₂NP

Chemical Property:

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Technology Process of C₂₁H₂₂NP

There total 2 articles about C₂₁H₂₂NP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6274-57-3
(4-bromobenzyl)dimethylamine

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1390631-77-2
C₂₁H₂₂NP

Guidance literature:: (4-bromobenzyl)dimethylamine; With tert.-butyl lithium; In pentane; at -78 ℃; for 2h; Schlenk technique; Inert atmosphere;

chloro-diphenylphosphine; In pentane; at 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1002/cssc.201403397

Reference yield:

: 589-15-1
1-bromomethyl-4-bromobenzene

: 1390631-77-2
C₂₁H₂₂NP

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / water; tetrahydrofuran / 24 h / 60 °C / Inert atmosphere

2.1: magnesium / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 2 h / 0 - 20 °C / UV-irradiation

With potassium carbonate; magnesium; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2013.03.021