m-hydroxyethynyl benzene

Base Information

• Chemical Name: m-hydroxyethynyl benzene
• CAS No.: 104170-24-3
• Molecular Formula: C₈H₆O
• Molecular Weight: 118.135

Synonyms:m-hydroxyethynyl benzene

Chemical Property of m-hydroxyethynyl benzene

Chemical Property:

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Technology Process of m-hydroxyethynyl benzene

There total 3 articles about m-hydroxyethynyl benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.8%

4-chloro-2-methylbut-3-yn-2-ol (29552-15-6) + phenylmagnesium bromide → biphenyl (92-52-4,1594-86-1) + m-hydroxyethynyl benzene (104170-24-3)

Guidance literature:

In toluene;

DOI:10.1023/A:1012348627878

Reference yield:

2-hydroxy-3-phenylcyclopropenone (1600-39-1) → m-hydroxyethynyl benzene (104170-24-3)

Guidance literature:

In methanol; Quantum yield; Photolysis;

DOI:10.1021/jo034869m

Reference yield:

→ m-hydroxyethynyl benzene (104170-24-3)

Guidance literature:

upstream raw materials:

4-chloro-2-methylbut-3-yn-2-ol

2-hydroxy-3-phenylcyclopropenone

Downstream raw materials:

4-(3-ethynylphenoxy)-o-dinitrobenzene

phenylketene

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