(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid

Base Information

• Chemical Name: (4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid
• CAS No.: 191276-32-1
• Molecular Formula: C₂₅H₂₃NO₆
• Molecular Weight: 433.461

Synonyms:(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid

Chemical Property of (4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid

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Technology Process of (4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid

There total 1 articles about (4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl-(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylate → (4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid (191276-32-1)

Guidance literature:

With lithium hydroxide; In ethanol; water; at 22 ℃; for 0.333333h;

Reference yield: 68.0%

(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid (191276-32-1) + 7-O-triethylsilyl-10-deacetoxy-13-deoxy-13-imino baccatin III (178329-27-6) → 7-O-triethylsilyl-10-deacetoxy-13,14ene-13-deoxy-13-(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-oxazolidin-5-yl-carbonylamino baccatin III + 7-O-triethylsilyl-10-deacetoxy-13-deoxy-13-(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-oxazolidin-5-yl-carbonylimino baccatin III

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In toluene; at 22 ℃; for 0.5h;

Reference yield: 54.0%

(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid (191276-32-1) + C36H50O11Si (423176-37-8) → Benzoic acid (2aR,4S,4aS,6R,10S,10aR,10bS)-6,10b-diacetoxy-7-[2-((2R,3S)-3-benzoylamino-2-hydroxy-3-phenyl-propionyloxy)-1-methyl-eth-(E)-ylidene]-4-hydroxy-4a,8,8-trimethyl-5,9-dioxo-dodecahydro-2-oxa-cyclobuta[3,4]benzo[1,2]cycloocten-10-yl ester

Guidance literature:

(4S,5R)-N-benzoyl-2-(2,4-dimethoxyphenyl)-4-phenyl-5-oxazolidine carboxylic acid; C₃₆H₅₀O₁₁Si; With dmap; dicyclohexyl-carbodiimide; In toluene; at 20 ℃; for 1h;

With hydrogenchloride; acetic anhydride; In methanol;

DOI:10.1002/1099-0690(20021)2002:2<277::AID-EJOC277>3.0.CO;2-F

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