Technology Process of C26H31BN4O9
There total 6 articles about C26H31BN4O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H25BO6;
With
dmap; dicyclohexyl-carbodiimide;
In
acetonitrile;
at 0 ℃;
for 0.5h;
Inert atmosphere;
2-((7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino)ethanol;
In
acetonitrile;
at 20 ℃;
for 22h;
Inert atmosphere;
DOI:10.1039/c3cc47534d
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetone / 2 h / Reflux
1.2: 20 h / Reflux
2.1: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C
3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium acetate / 1,4-dioxane / 4 h / 95 °C / Inert atmosphere
4.1: trifluoroacetic acid / water / 3 h / 90 °C
5.1: dicyclohexyl-carbodiimide; dmap / acetonitrile / 0.5 h / 0 °C / Inert atmosphere
5.2: 22 h / 20 °C / Inert atmosphere
With
dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium acetate; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
1,4-dioxane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
3.1: |Miyaura Borylation Reaction;
DOI:10.1039/c3cc47534d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / acetonitrile / 0.5 h / 20 °C / Inert atmosphere
2.1: dicyclohexyl-carbodiimide; dmap / acetonitrile / 0.5 h / 0 °C / Inert atmosphere
2.2: 22 h / 20 °C / Inert atmosphere
With
dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
acetonitrile;
DOI:10.1039/c3cc47534d
