cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid

Base Information

• Chemical Name: cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid
• CAS No.: 850227-76-8
• Molecular Formula: C₉H₁₀ClF₃O₂
• Molecular Weight: 242.625
• Mol file: 850227-76-8.mol

Synonyms:cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid

Chemical Property of cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid

There total 2 articles about cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid (850227-76-8) + cyclopropanecarboxylic acid (1759-53-1)

Guidance literature:

Reference yield:

→ 3-[(Z)-2-chloro-3,3,3-trifluoroprop-1-enyl]-2,2-dimethylcyclopropanecarbonyl chloride (393870-46-7,68127-98-0,76496-71-4) + cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid (850227-76-8)

Guidance literature:

Reference yield: 95.0%

toluene-4-sulfonic acid 5-phenylpent-4-ynyl ester + cis-3-(2-chloro-3,3,3-trifluoroprop-1-ene-1-yl)-2,2-dimethylcyclopropanecarboxylic acid (850227-76-8) → 5-phenylpent-4-yn-1-yl (Z)-3-(2-chloro-3,3,3-trifluoroprop-1-en-1-yl)-2,2-dimethylcyclopropane-1-carboxylate

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 1h; Schlenk technique;

DOI:10.1039/d1gc03187b

Downstream raw materials:

3-[(Z)-2-chloro-3,3,3-trifluoroprop-1-enyl]-2,2-dimethylcyclopropanecarbonyl chloride

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