6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol

Base Information

Chemical Name:6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol
CAS No.:1027360-77-5
Molecular Formula:C₁₉H₁₈ClF₃N₂O₃S
Molecular Weight:446.878
Hs Code.:

Synonyms:6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol

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Technology Process of 6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol

There total 2 articles about 6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027348-97-5
3-tert-butyl-5-chloro-2-hydroxy-6-methyl-benzoic acid phenyl ester

: 2355-16-0
4-trifluoromethanesulfonyl-benzene-1,2-diamine

: 1027360-77-5
6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol

Guidance literature:: 3-tert-butyl-5-chloro-2-hydroxy-6-methyl-benzoic acid phenyl ester; 4-trifluoromethanesulfonyl-benzene-1,2-diamine; In N,N-dimethyl-formamide; at 150 ℃; for 1.5h; microwave irradiation;

With acetic acid; In N,N-dimethyl-formamide; at 200 ℃; for 1 - 2h; microwave irradiation;

Reference yield:

: 1027345-71-6
3-tert-butyl-5-chloro-2-hydroxy-6-methyl-benzaldehyde

: 2355-16-0
4-trifluoromethanesulfonyl-benzene-1,2-diamine

: 1027360-77-5
6-tert-butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)phenol

Guidance literature:: 3-tert-butyl-5-chloro-2-hydroxy-6-methyl-benzaldehyde; 4-trifluoromethanesulfonyl-benzene-1,2-diamine; In acetonitrile; at 90 ℃; for 18h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; at 70 ℃; Product distribution / selectivity;