C₅₈H₇₆ClN₁₁O₁₄

Base Information

Chemical Name:C₅₈H₇₆ClN₁₁O₁₄
CAS No.:859236-16-1
Molecular Formula:C₅₈H₇₆ClN₁₁O₁₄
Molecular Weight:1186.76
Hs Code.:

C<sub>58</sub>H<sub>76</sub>ClN<sub>11</sub>O<sub>14</sub>

Synonyms:C₅₈H₇₆ClN₁₁O₁₄

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Chemical Property of C₅₈H₇₆ClN₁₁O₁₄

Chemical Property:

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Technology Process of C₅₈H₇₆ClN₁₁O₁₄

There total 27 articles about C₅₈H₇₆ClN₁₁O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-amino-N-[5-sec-butyl-18,19-dimethyl-11-(2-nitro-cyclopropylmethyl)-4,7,10,13,16,20-hexaoxo-8,14-bis-(1-phenyl-ethyl)-2-propenyl-eicosahydro-3a,6,9,12,15,19-hexaaza-cyclopentacyclononadecen-17-yl]-3-(2-nitro-cyclopropyl)-propionamide

: 802911-30-4
5-chloro-1-(methoxymethoxy)-1H-pyrrole-2-carboxylic acid

: 859236-16-1
C₅₈H₇₆ClN₁₁O₁₄

Guidance literature:: With 2,4,6-trimethyl-pyridine; 1-hydroxy-7-aza-benzotriazole; HATU; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1002/chem.200400977

Reference yield:

: (S)-3-((1R,2R)-2-Nitro-cyclopropyl)-2-(2-trimethylsilanyl-ethoxycarbonylamino)-propionic acid; compound with cyclohexylamine

: 859236-16-1
C₅₈H₇₆ClN₁₁O₁₄

Guidance literature:: Multi-step reaction with 3 steps

1: 32.5 mg / O-(7-azabenzotriazole-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 7-aza-1-hydroxybenzotriazole; 2,4,6-trimethylpyridine / i-Pr₂NEt / CH₂Cl₂ / 15 h / 20 °C

2: TFA / 1 h / 20 °C

3: 25.0 mg / O-(7-azabenzotriazole-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 7-aza-1-hydroxybenzotriazole; 2,4,6-trimethylpyridine / i-Pr₂NEt / CH₂Cl₂ / 4 h / 20 °C

With 2,4,6-trimethyl-pyridine; 1-hydroxy-7-aza-benzotriazole; HATU; trifluoroacetic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/chem.200400977

Reference yield:

: 859235-88-4
(2R,3R)-2-tert-Butoxycarbonylamino-3-methylamino-butyric acid methyl ester

: 859236-16-1
C₅₈H₇₆ClN₁₁O₁₄

Guidance literature:: Multi-step reaction with 14 steps

1: 0.135 g / 2,4,6-trimethylpyridine; 7-aza-1-hydroxybenzotriazole / ethyl acetate / 15 h / 20 °C

2: aq. HCl / ethyl acetate / 3 h / 20 °C

3: 0.122 g / 2,4,6-trimethylpyridine; i-Pr₂NEt / acetonitrile / 16 h / 20 °C

4: Et₂NH / acetonitrile / 0.67 h / 20 °C

5: 0.104 mg / N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide hydrochloride; 7-aza-1-hydroxybenzotriazole; 2,4,6-trimethylpyridine / CH₂Cl₂ / 16 h / 20 °C

6: 73 percent / aq. tetra-n-butylammonium hydroxide / tetrahydrofuran / 0.75 h / 0 °C

7: 93 percent / O-(7-azabenzotriazole-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 7-aza-1-hydroxybenzotriazole; 2,4,6-trimethylpyridine / i-Pr₂NEt / CH₂Cl₂ / 15 h / 20 °C

8: 98 percent / Bu₄N(+)F(-) / acetonitrile / 2 h / 20 - 55 °C

9: aq. HCl / ethyl acetate / 1 h / 20 °C

10: 31.6 mg / O-(7-azabenzotriazole-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 7-aza-1-hydroxybenzotriazole; i-Pr₂NEt / CH₂Cl₂ / 22 h / 20 °C

11: anisole; TFA / 2 h / 20 °C

12: 32.5 mg / O-(7-azabenzotriazole-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 7-aza-1-hydroxybenzotriazole; 2,4,6-trimethylpyridine / i-Pr₂NEt / CH₂Cl₂ / 15 h / 20 °C

13: TFA / 1 h / 20 °C

14: 25.0 mg / O-(7-azabenzotriazole-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 7-aza-1-hydroxybenzotriazole; 2,4,6-trimethylpyridine / i-Pr₂NEt / CH₂Cl₂ / 4 h / 20 °C

With 2,4,6-trimethyl-pyridine; hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydroxide; methoxybenzene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1002/chem.200400977