1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione

Base Information

• Chemical Name: 1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione
• CAS No.: 6129-68-6
• Molecular Formula: C₃₁H₂₃N₅O₁₅
• Molecular Weight: 705.548

Synonyms:1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione

Chemical Property of 1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione

Chemical Property:

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Technology Process of 1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione

There total 2 articles about 1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

bis(trimethylsilyloxy)pyrimidine (68027-39-4) + 2-deoxy-1,3,4,6-tetrakis-O-(4-nitrobenzoyl)-α-D-ribo-hexopyranose (107796-01-0) → 1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione (6129-68-6)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; for 2h; Heating;

DOI:10.1021/jm00389a015

Reference yield:

→ 1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione (6129-68-6)

Guidance literature:

1-(2-Desoxy-O³,O⁴,O⁶-tri-4-nitrobenzoyl-β-D-ribo-hexosyl)-4-aethoxy-(1H)-pyrimidin-2-on, methanol HCl, CH2Cl2;

DOI:10.1021/jo01022a518

Reference yield: 76.0%

1-(2-deoxy-3,4,6-tris-O-(4-nitrobenzoyl)-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione (6129-68-6) → 1-(2-deoxy-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione (6067-31-8)

Guidance literature:

With sodium methylate; In methanol; for 2h;

DOI:10.1021/jm00389a015

upstream raw materials:

bis(trimethylsilyloxy)pyrimidine

2-deoxy-1,3,4,6-tetrakis-O-(4-nitrobenzoyl)-α-D-ribo-hexopyranose

Downstream raw materials:

1-(2-deoxy-β-D-ribo-hexopyranosyl)-2,4-pyrimidinedione

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