Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester

Base Information

Chemical Name:Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester
CAS No.:82825-41-0
Molecular Formula:C₃₇H₂₄Cl₁₄N₃O₅
Molecular Weight:1086.96
Hs Code.:

Synonyms:Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester

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Chemical Property of Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester

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Technology Process of Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester

There total 3 articles about Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 77225-19-5
Tetradecachloro-4-(chlorocarbonyl)triphenylmethyl Radical

: 82825-40-9
glycylglycylphenylalanine tert-butyl ester

: 82825-41-0
Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester

Guidance literature:: With triethylamine; In dichloromethane; for 29h; Ambient temperature;
DOI:10.1021/jo00169a021

Reference yield:

: 82825-39-6
N-(Benzyloxycarbonyl)glycylglycylphenylalanine tert-butyl ester

: 82825-41-0
Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.076 g / H₂ / Pd/C / methanol; H₂O / 5 h / Ambient temperature

2: 45 percent / triethylamine / CH₂Cl₂ / 29 h / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1021/jo00169a021

Reference yield:

: 77212-86-3
(tetradecachloro-4-carboxytriphenyl)methyl radical

: 82825-41-0
Tetradecachloro-4-(phenylalaninoglycinoglycinocarbonyl)triphenylmethyl Radical tert-Butyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / SOCl₂ / 24 h / Heating; other reagent: PCl₅ and POCl₃

2: 45 percent / triethylamine / CH₂Cl₂ / 29 h / Ambient temperature

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo00169a021