benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate

Base Information

Chemical Name:benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate
CAS No.:871565-54-7
Molecular Formula:C₂₄H₂₆N₂O₃
Molecular Weight:390.482
Hs Code.:

Synonyms:benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate

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Chemical Property of benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate

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Technology Process of benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate

There total 1 articles about benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869337-75-7
benzyl 3,5-dimethyl-4-(ethanoic acid)pyrrole-2-carboxylate

: 2627-86-3
(S)-1-phenyl-ethylamine

: 871565-54-7
benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate

Guidance literature:: With dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In tetrahydrofuran; at 20 ℃; for 48h;
DOI:10.1021/jo051727e

Reference yield:

: 871565-54-7
benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate

: 3,5-dimethyl-4-[(1-phenyl-ethylcarbamoyl)-methyl]-1H-pyrrole-2-carboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 16h;
DOI:10.1021/jo051727e

Reference yield:

: 871565-54-7
benzyl 3,5-dimethyl-4-[(S)-2-(1-phenylethylcarbamoyl)methyl]-1H-pyrrole-2-carboxylate

: C₄₇H₅₄N₆O₂*2BrH

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / tetrahydrofuran / 16 h

2: HBr / tetrahydrofuran; methanol; H₂O / 0.33 h

With hydrogen bromide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo051727e