bis-(m-tolyl)phenylphosphane oxide

Base Information

Chemical Name:bis-(m-tolyl)phenylphosphane oxide
CAS No.:18803-10-6
Molecular Formula:C₂₀H₁₉OP
Molecular Weight:306.344
Hs Code.:

Synonyms:bis-(m-tolyl)phenylphosphane oxide

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Chemical Property of bis-(m-tolyl)phenylphosphane oxide

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Technology Process of bis-(m-tolyl)phenylphosphane oxide

There total 9 articles about bis-(m-tolyl)phenylphosphane oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 145290-34-2
bis(3-methylphenyl)phosphine oxide

: 18803-10-6
bis-(m-tolyl)phenylphosphane oxide

Guidance literature:: With copper(l) iodide; cesium fluoride; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.joc.6b01776

Reference yield: 96.0%

: 18803-08-2
bis(3-methylphenyl)phenylphosphine

: 18803-10-6
bis-(m-tolyl)phenylphosphane oxide

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1002/chem.201002073

Reference yield: 22.0%

: 625-95-6
3-Iodotoluene

: 791-28-6
Triphenylphosphine oxide

: 18803-10-6
bis-(m-tolyl)phenylphosphane oxide

: 6840-27-3
(3-methylphenyl)diphenylphosphine oxide

: 6151-88-8
tri(m-tolyl)phosphine oxide

Guidance literature:: 3-Iodotoluene; With n-butyllithium; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 2h; Inert atmosphere; Schlenk technique;

Triphenylphosphine oxide; In diethyl ether; hexane; cyclohexane; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2015.12.043