4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile

Base Information

Chemical Name:4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile
CAS No.:214485-18-4
Molecular Formula:C₂₂H₁₃ClN₄O₂S
Molecular Weight:432.89
Hs Code.:

Synonyms:4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile

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Chemical Property of 4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile

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Technology Process of 4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile

There total 4 articles about 4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32631-26-8
4-amino-2-chlorophenyl phenyl sulphide

: 214470-37-8
4-chloro-6-nitro-3-quinolinecarbonitrile

: 214485-18-4
4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile

Guidance literature:: 4-amino-2-chlorophenyl phenyl sulphide; 4-chloro-6-nitro-3-quinolinecarbonitrile; In ethanol; for 8h; Heating / reflux;

With sodium hydrogencarbonate; In ethanol; water;

Reference yield:

: 2458-24-4
2-cyano-3-(4-nitro-phenylamino)-acrylic acid ethyl ester

: 214485-18-4
4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl ether-biphenyl eutectic / 12.5 h / 260 °C

2: trichlorophosphate / 5.5 h / Heating / reflux

3: ethanol / 8 h / Heating / reflux

With diphenyl ether-biphenyl eutectic; trichlorophosphate; In ethanol;

Reference yield:

: 214470-35-6,2305-65-9
6-nitro-4-oxo-1,4-dihydro-quinoline-3-carbonitrile

: 214485-18-4
4-[(3-chloro-4-thiophenoxy)phenylamino]-6-nitro-quinoline-3-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 5.5 h / Heating / reflux

2: ethanol / 8 h / Heating / reflux

With trichlorophosphate; In ethanol;