N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide
CAS No.:1217009-19-2
Molecular Formula:C₁₄H₁₉ClN₂O₂S
Molecular Weight:314.836
Hs Code.:

Synonyms:N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

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Technology Process of N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

There total 1 articles about N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 10409-46-8
2-chloro-2-methylcyclohexanone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1217009-19-2
N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: In diethyl ether; for 12h; Inert atmosphere;
DOI:10.1021/ja100932q

Reference yield: 86.0%

: 1217009-19-2
N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

: 925-90-6
ethylmagnesium bromide

: 1217009-41-0
N'-(2-ethyl-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: ethylmagnesium bromide; With copper(l) chloride; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide; In tetrahydrofuran; at -78 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja100932q

Reference yield: 74.0%

: 1217009-51-2
(1-methylcyclopentyl)magnesium chloride

: 1217009-19-2
N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide

: 1217009-52-3
4-methyl-N'-(2-methyl-2-(1-methylcyclopentyl)cyclohexylidene)benzenesulfonohydrazide

Guidance literature:: (1-methylcyclopentyl)magnesium chloride; With copper(l) chloride; In tetrahydrofuran; at -30 ℃; for 0.5h; Inert atmosphere;

N'-(2-chloro-2-methylcyclohexylidene)-4-methylbenzenesulfonohydrazide; In tetrahydrofuran; at -30 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja100932q